Jpn. J. Appl. Phys. 44 (2005) pp. 4194-4199 |Previous Article| |Next Article| |Table of Contents|
|Full Text PDF (140K)| |Buy This Article|
High-Field NMR up to 30 T with a Hybrid Magnet
Kenjiro Hashi,
Tadashi Shimizu,
Atsushi Goto,
Takahiro Iijima and
Shinobu Ohki
National Institute for Materials Science, Sakura, Tsukuba, Ibaraki 305-0003, Japan
(Received January 14, 2005; accepted February 23, 2005; published June 10, 2005)
NMR measurements up to 30 T were performed with the hybrid magnet installed in the National Institute for Materials Science (NIMS). The field profile and stability of superconducting, resistive and their hybrid magnets were measured using 63Cu NMR of a Cu metal. The field homogeneity of the hybrid magnet at 30 T is 186±4 ppm in the region ±5 mm from the field center along the z-axis. The magnetic field fluctuates with a total amplitude of about 30 G at 30 T (100 ppm). The present status of the hybrid magnet for high-resolution solid-state NMR measurements is discussed.
URL:
http://jjap.jsap.jp/link?JJAP/44/4194/
DOI: 10.1143/JJAP.44.4194
- K. Wüthrich: Nat. Struct. Biol. 5 (1998) 492.
- Z. Gan, P. Gor'kov, T. A. Cross, A. Samoson and D. Massiot:
J. Am. Chem. Soc. 124 (2002) 5634[CrossRef].
- L. Frydman and J. S. Harwood:
J. Am. Chem. Soc. 117 (1995) 5367[CrossRef].
- A. Samoson, E. Lippmaa and A. Pines: Mol. Phys. 65 (1988) 1013.
- K. T. Mueller, B. Q. Sun, G. C. Chingas, J. W. Zwanziger, T. Terao and A. Pines: J. Magn. Reson. 86 (1990) 470.
- Z. H. Gan:
J. Chem. Phys. 114 (2001) 10845[AIP Scitation].
- T. Kiyoshi et al.:
IEEE Trans. Appl. Supercond. 11 (2001) 2347[CrossRef].
- K. Hashi, T. Shimizu, A. Goto, T. Kiyoshi, S. Matsumoto, H. Wada, T. Fujito, K. Hasegawa, M. Yoshikawa, T. Miki, S. Ito, M. Hamada and S. Hayashi: J. Magn. Reson. 156 (2002) 318.
- Very recentry, 930 MHz (21.9 T) operation was achieved.
- M. D. Bird, S. Bole, Y. M. Eyssa, H.-J. Schneider-Muntau, T. Kiyoshi, T. Asano, Y. Sakai, K. Inoue and H. Wada: Proc. MT-15, 1997, p. 664.
- K. Hashi, A. Goto, T. Shimizu, T. Iijima and S. Ohki:
Physica B 346–347 (2004) 531[CrossRef].
- T. Shimizu, A. Goto, K. Hashi and S. Ohki:
IEEE Trans. Appl. Supercond. 14 (2004) 1632[CrossRef].
- K. Inoue, T. Kiyoshi, M. Kosuge, T. Takeuchi, F. Matsumoto, H. Maeda, S. Hanai, M. Tezuka and K. Matsutani: IEEE Trans. Magn. 32 (1996) 2450.
- S. Hosoya, K. Inokuchi, T. Suzuki, T. Goto, H. Tanaka, S. Awaji, K. Watanabe, T. Sasaki, T. Fukase, T. Shimizu and A. Goto:
Physica B 329–333 (2003) 977[CrossRef].
- P. L. Kuhns, A. Kleinhammes, W. G. Moulton and N. S. Sullivan: J. Magn. Reson. A 115 (1995) 270.
- K. Kodama, M. Takigawa, M. Horvatić, C. Berthier, H. Kageyama, Y. Ueda, S. Miyahara, F. Becca and F. Mila: Science 298 (2002) 395[Science].
- W. G. Clark, P. Vonlanthen, A. Goto, K. B. Tanaka, B. Alavi, W. G. Moulton, A. Reyes and P. Kuhns: Int. J. Mod. Phys. B 16 (2002) 3252.
- G.-q. Zheng, H. Ozaki, Y. Kitaoka, P. Kuhns, A. P. Reyes and W. G. Moulton:
Phys. Rev. Lett. 88 (2002) 077003[APS].
- K. Hashi, T. Shimizu, A. Goto, T. Iijima and S. Ohki:
Jpn. J. Appl. Phys. 43 (2004) L1020[JSAP].
- V. Soghomonian, M. Sabo, A. Powell, P. Murphy, R. Rosanske, T. A. Cross and H. J. Schneider-Muntau:
Rev. Sci. Instrum. 71 (2000) 2882[AIP Scitation].